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Fujita, Yoshitaka; Seki, Misaki; Namekawa, Yoji*; Nishikata, Kaori; Daigo, Fumihisa; Ide, Hiroshi; Tsuchiya, Kunihiko; Sano, Tadafumi*; Fujihara, Yasuyuki*; Hori, Junichi*; et al.
KURNS Progress Report 2020, P. 136, 2021/08
no abstracts in English
Matsueda, Makoto; Yanagisawa, Kayo*; Koarai, Kazuma; Terashima, Motoki; Fujiwara, Kenso; Abe, Hironobu; Kitamura, Akihiro; Takagai, Yoshitaka*
ACS Omega (Internet), 6(29), p.19281 - 19290, 2021/07
Times Cited Count:2 Percentile:14.88(Chemistry, Multidisciplinary)Online solid-phase extraction-inductively coupled plasma-quadrupole mass spectrometry with oxygen dynamic reaction cell (online SPE-ICP-MS-DRC) was shown to be a thorough automatic analytical system, circumventing the need for human handling. At three stepwise separations (SPE-DRC-Q mass filters), we showed that interference materials allowed the coexistence of abundance ratios of 1.510 for Tc/Mo. Using this optimized system, a detection limit of Tc was 9.3 pg/L (5.9 mBq/L) for a 50 mL injection and sequential measurements were undertaken at a cycle of 24 min/sample.
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Journal of Radioanalytical and Nuclear Chemistry, 102(2), p.533 - 550, 1986/02
Times Cited Count:8 Percentile:66.77(Chemistry, Analytical)no abstracts in English
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JAERI-M 85-066, 22 Pages, 1985/06
no abstracts in English
Ueno, Kaoru
Nihon Kagaku Zasshi, 90(7), p.718 - 719, 1969/00
no abstracts in English
Matsueda, Makoto; Terashima, Motoki; Takagai, Yoshitaka*
no journal, ,
Technetium-99 (Tc) is a pure beta-emitting radionuclide with a long half-life (210 000 years), produced with a yield of about 6% during the fission of U and Pu. The properties of high mobility in environment and concentrated into specific seaweeds were applied as a tracer for radioisotopes released into the environment. Inductively coupled plasma-mass spectrometry (ICP-MS) is the main method for Tc analysis; however, the isobars (Ru and MoH) interfere the quantification. In this study, a multi-stage separation and analysis system (online SPE-ICP-MS) for Tc was constructed by attaching a solid phase extraction (SPE) resin to a flow injection (FI) system and combining it with a collision reaction cell (CRC) in an ICP-MS. In addition, a high sensitivity for detecting trace amounts of Tc was developed.
Matsueda, Makoto
no journal, ,
no abstracts in English